TY - JOUR
T1 - Engineering in ceramic albite morphology by the addition of additives
T2 - Carbon nanotubes and graphene oxide for energy applications
AU - Ur Rehman, Zia
AU - Yao, Shanshan
AU - Nazir, Muhammad Altaf
AU - Ullah, Hameed
AU - Aziz, Irum
AU - Blel, Asma
AU - Karim, Mohammad R.
AU - Hanif, Muhammad Bilal
AU - Munir, Mamona
AU - Park, Dong Yong
AU - Choi, Dongwhi
N1 - Publisher Copyright:
© 2024 the author(s), published by De Gruyter.
PY - 2024/1/1
Y1 - 2024/1/1
N2 - The synthesis of zeolite nanoparticles is studied comprehensively by adding an organic template as a reflux method, extracted from crystals. The zeolite nano-crystals are quite effectively synthesized by incorporating silica, organic template, and alkali metal. The tetrapropylammoniumhydroxide, tetrapropylammoniumbromide and tetraethyl orthosilicate (TEOS) as organic templates are added for the assistance of zeolite (albite) crystals. A cross-linker TEOS is also mixed. Adding carbon nanotubes and graphene oxide made the morphology of albite more interesting. Nucleation time is an important feature for the formation of albite crystals. The albite nano-shaped crystal is developed for instance when reaction time is less than 240 h, after this period crystal size increases with time. Batch 1 of zeolite is prepared with additives for testing its morphology, like surface area, particle size shape, and crystal geometry. The general trend (e.g., pore volume, percentage composition, particle size, geometry) of zeolite nano-crystal is explained by the help of robust techniques such as Fourier transform infrared spectroscopy, X-ray diffraction, Brunauer–Emmett–Teller, energy-dispersive X-ray spectroscopy, and scanning electron microscopy.
AB - The synthesis of zeolite nanoparticles is studied comprehensively by adding an organic template as a reflux method, extracted from crystals. The zeolite nano-crystals are quite effectively synthesized by incorporating silica, organic template, and alkali metal. The tetrapropylammoniumhydroxide, tetrapropylammoniumbromide and tetraethyl orthosilicate (TEOS) as organic templates are added for the assistance of zeolite (albite) crystals. A cross-linker TEOS is also mixed. Adding carbon nanotubes and graphene oxide made the morphology of albite more interesting. Nucleation time is an important feature for the formation of albite crystals. The albite nano-shaped crystal is developed for instance when reaction time is less than 240 h, after this period crystal size increases with time. Batch 1 of zeolite is prepared with additives for testing its morphology, like surface area, particle size shape, and crystal geometry. The general trend (e.g., pore volume, percentage composition, particle size, geometry) of zeolite nano-crystal is explained by the help of robust techniques such as Fourier transform infrared spectroscopy, X-ray diffraction, Brunauer–Emmett–Teller, energy-dispersive X-ray spectroscopy, and scanning electron microscopy.
KW - albite
KW - CNTs
KW - graphene oxide
KW - surface morphology
KW - synthesis
UR - http://www.scopus.com/inward/record.url?scp=85198341852&partnerID=8YFLogxK
U2 - 10.1515/ntrev-2023-0221
DO - 10.1515/ntrev-2023-0221
M3 - Article
AN - SCOPUS:85198341852
SN - 2191-9089
VL - 13
JO - Nanotechnology Reviews
JF - Nanotechnology Reviews
IS - 1
M1 - 20230221
ER -